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Hydrothermal carbonization is a thermochemical process for the pretreatment of high moisture content biomass under hot compressed water, making it applicable for diversified purposes. It is performed in a closed reactor at a temperature range of 180–280°C under pressure (2–6 MPa) for 5 to 240 min ( Arellano et al., 2016 ).
Jan 01, 2022 · The reactions that take place during liquefaction are: hydrolysis, conversion by decarboxylation and dehydration, and rearrangement via condensation, cyclization, and polymerization yielding hydrophobic macromolecules (Gollakota et al., 2018). As aforementioned, the HTL products are composed of a biocrude-oil, aqueous and gaseous …
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Aug 09, 2021 · A modern pulp mill generates a variety of different by-products and waste streams, some of these can be recycled, refined, sold, or used on-site for energy production. However, some, such as chemical and biological sludges produced in wastewater treatment cannot be reused or disposed of easily, mainly due to their high moisture content and poor drying …
The saturated fatty acids (stearic, palmitic, and lauric acid) gave the corresponding decarboxylation products (n-alkanes) with gre … Hydrothermal decarboxylation and hydrogenation of fatty acids over Pt/C ChemSusChem. 2011 Apr 18;4(4):481-6. doi: 10.1002/cssc.201000370. Epub 2011 Jan 27. Authors Jie Fu 1 ...
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Apr 23, 2021 · This work describes batch-type hydrothermal liquefaction (HTL) treatments of conifer wood chips at 180–425 °C, under either air or nitrogen atmosphere. Such experiments allow efficient extraction of 5-hydroxymethyl furfural (HMF) and other valuable chemical substances, such as glycolic acid and acetic acid, from the lignocellulosic biomass. These …
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1000ml series Hydrothermal Synthesis Reactor KH series Hydrothermal synthesis reactor is used in catalysis, crystal, polymer and other experiments, it adopts the external heating mode. In order to reduce the size, and be suitable for several reaction kettles working at the same time and same reaction temperature (for example, put several ...
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The hydrothermal reactor is mainly made up of two parts; an outer high-quality stainless-steel jacket and an inner Teflon liner or Teflon chamber. In the Teflon-lined autoclave, the reaction is carried out at a maximum 240-degree Celsius (428 Fahrenheit), while the safe temperature is 200-degree Celsius (392 Fahrenheit).
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Oct 01, 2013 · The catalytic hydrothermal decarboxylation of stearic acid over Pt/MWCNTs, Pt/C and Ru/C were carried out with 0.176 mmol of stearic acid and 10 mg of catalyst at 330 °C for 30 min.The conversions of stearic acid for stearic acid decarboxylation over Pt/MWCNTs, Pt/C and Ru/C were 52.4 ± 2.4%, 52.4 ± 2.5% and 42.3 ± 5.2%, respectively.
Apr 18, 2022 · The reactor was purged with helium to remove air from the reactor headspace before being sealed. When the reactor reached the required temperature (400 °C), the reaction was maintained for 60 min, then removed and cooled using a fan, allowing the reaction products to be collected and separated as described previously [ 16 ].
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