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Apr 19, 2021 · After your newly decarboxylated oil has sat at temp for an hour, lower the temperature setting of the jacket to 85°C (185°F) and allow the mixture to cool to at least 90°C (194°F) before discharging the oil from the vessel. You can then introduce atmosphere and drain the oil into your tertiary container. The purpose of this step is to avoid ...
Jun 13, 2016 · The decarboxylation of fatty acids was carried out in a micro batch reactor (1.67 mL volume), which was assembled from one 3/8-inch tube and two 3/8-inch caps purchased from Swagelok, USA. The photo of the micro batch reactor and its parts is shown in Fig. 1. A certain amount of reactant and catalyst were added to the reactor.
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We report herein on the conversion of saturated and unsaturated fatty acids to alkanes over Pt/C in high-temperature water. The reactions were done with no added H (2) . The saturated fatty acids (stearic, palmitic, and lauric acid) gave the corresponding decarboxylation products (n-alkanes) with greater than 90 % selectivity, and the formation ...
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Hydrothermal carbonization is a thermochemical process for the pretreatment of high moisture content biomass under hot compressed water, making it applicable for diversified purposes. It is performed in a closed reactor at a temperature range of 180–280°C under pressure (2–6 MPa) for 5 to 240 min ( Arellano et al., 2016 ).
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May 01, 2001 · The reactor is 1.1 l jacketed glass vessel. Tap water is used as the coolant on the jacket. To heat the mixture in the reactor an electrical heater which is connected with a thyristor is used. To bubble nitrogen through the reaction mixture during the experiments a tube was inserted through one of the reactor head ports.
Jan 30, 2014 · Hydrothermal carbonization. Hydrothermal carbonization of loblolly pine was performed in a 100 -mL Parr bench top reactor (Moline, IL). Nitrogen of 80 cm 3 (STP) min −1 was first passed through the reactor for 10 min to purge oxygen. For each run, a 1:5 mass ratio mixture of loblolly pine to water was loaded into the reactor, while ensuring ...
Hydrothermal carbonization is a thermochemical process for the pretreatment of high moisture content biomass under hot compressed water, making it applicable for diversified purposes. It is performed in a closed reactor at a temperature range of 180–280°C under pressure (2–6 MPa) for 5 to 240 min ( Arellano et al., 2016 ).
Dec 28, 2020 · Typically, the reaction mechanisms of hydrothermal carbonization mainly include hydrolysis, dehydration, decarboxylation, aromatization, and condensation polymerization (Funke and Ziegler, 2010). As water is used as reaction medium and acts as a catalyst during HTC process, the pre-drying step is unnecessary in HTC, indicating that HTC is more ...
Apr 23, 2021 · This work describes batch-type hydrothermal liquefaction (HTL) treatments of conifer wood chips at 180–425 °C, under either air or nitrogen atmosphere. Such experiments allow efficient extraction of 5-hydroxymethyl furfural (HMF) and other valuable chemical substances, such as glycolic acid and acetic acid, from the lignocellulosic biomass. These …
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Nov 24, 2019 · This work describes an approach towards experimental implementation of real time control studies conducted on a batch polymerization reactor. The information is related to the controlling of molecular weight for styrene acrylonitrile copolymer polymerization system in a batch reactor generated under a varied range of temperatures, reactant concentrations and …
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