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Jan 30, 2014 · Hydrothermal carbonization. Hydrothermal carbonization of loblolly pine was performed in a 100 -mL Parr bench top reactor (Moline, IL). Nitrogen of 80 cm 3 (STP) min −1 was first passed through the reactor for 10 min to purge oxygen. For each run, a 1:5 mass ratio mixture of loblolly pine to water was loaded into the reactor, while ensuring ...
Apr 23, 2021 · This work describes batch-type hydrothermal liquefaction (HTL) treatments of conifer wood chips at 180–425 °C, under either air or nitrogen atmosphere. ... Several reactions occur during hydrothermal treatment, including hydrolysis, dehydration, decarboxylation, polymerization, ... Schematic diagram of a hydrothermal reactor. 1 = pressure ...
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Hydrothermal carbonization is a thermochemical process for the pretreatment of high moisture content biomass under hot compressed water, making it applicable for diversified purposes. It is performed in a closed reactor at a temperature range of 180–280°C under pressure (2–6 MPa) for 5 to 240 min ( Arellano et al., 2016 ).
Aug 09, 2021 · A modern pulp mill generates a variety of different by-products and waste streams, some of these can be recycled, refined, sold, or used on-site for energy production. However, some, such as chemical and biological sludges produced in wastewater treatment cannot be reused or disposed of easily, mainly due to their high moisture content and poor drying …
Jan 01, 2022 · The reactions that take place during liquefaction are: hydrolysis, conversion by decarboxylation and dehydration, and rearrangement via condensation, cyclization, and polymerization yielding hydrophobic macromolecules (Gollakota et al., 2018). As aforementioned, the HTL products are composed of a biocrude-oil, aqueous and gaseous …
This compound then underwent decarboxylation to form heptadecane. On the basis of these results, it appears that this reaction system promotes in situ H(2) formation. This hydrothermal decarboxylation route represents a new path for using renewable resources to make molecules with value as liquid transportation fuels.
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Oct 01, 2013 · The decarboxylation of fatty acids were carried out in a micro batch reactor (1.67 cm 3 volume), which was assembled from one 3/8-in. tube and two 3/8-in. caps purchased from Swagelok, USA. 0.176 mmol of reactant and 10 mg of 5% Pt/MWCNTs were added followed by loading certain amount of water in the reactor. In all experiments, the amount of ...
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Jan 01, 2022 · The reactions that take place during liquefaction are: hydrolysis, conversion by decarboxylation and dehydration, and rearrangement via condensation, cyclization, and polymerization yielding hydrophobic macromolecules (Gollakota et al., 2018). As aforementioned, the HTL products are composed of a biocrude-oil, aqueous and gaseous …
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The hydrothermal reactor is mainly made up of two parts; an outer high-quality stainless-steel jacket and an inner Teflon liner or Teflon chamber. In the Teflon-lined autoclave, the reaction is carried out at a maximum 240-degree Celsius (428 Fahrenheit), while the safe temperature is 200-degree Celsius (392 Fahrenheit).
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